Understanding the Principles of Organic Chemistry (gnv64)

Understanding the Principles of Organic Chemistry - A Laboratory Experience By Steven F. Pedersen, Arlyn M. Myers Brooks Cole | January 2010 | PDF | ISBN 10: 0495829935 | 432 pages | 16 mb Amazon Link : http://www.amazon.com/Understanding-Principles-Organic-Chemistry-Laboratory/dp/0495829935/ Class-tested by thousands of students and using simple equipment and green chemistry ideas, UNDERSTANDING THE PRINCIPLES OF ORGANIC CHEMISTRY: A LABORATORY COURSE includes 36 experiments that introduce traditional, as well as recently developed synthetic methods. Offering up-to-date and novel experiments not found in other lab manuals, this innovative book focuses on safety, gives students practice in the basic techniques used in the organic lab, and includes microscale experiments, many drawn from the recent literature. An Online Instructor's Manual available on the book's instructor's companion website includes helpful information, including instructors' notes, pre-lab meeting notes, experiment completion times, answers to end-of-experiment questions, video clips of techniques, and more. TABLE OF CONTENTS Preface to the Student xi Preface to the Instructor xiv The Front Cover: Nature’s Organic Chemistry Laboratory xix PART I Theory and Techniques Chapter 1 Safety in the Chemistry Laboratory 3 Chapter 2 The Laboratory Notebook and the Laboratory Period 9 Chapter 3 Where to Find It: Searching the Literature 13 Chapter 4 Things You Need to Know Before You Begin 15 Chapter 5 Properties of Organic Molecules 31 Chapter 6 Characteristic Physical Properties of Pure Compounds 53 Chapter 7 Isolation and Purification of Compounds 89 Chapter 8 Structure Determination 141 Chapter 9 Running a Synthetic Reaction 201 PART II Experiments Experiment 1 Calibrating a Pasteur Pipette 211 Experiment 2 Investigating Solubility and Acid-Base Reactions 214 Experiment 3 Mixed Melting Points 219 Experiment 4 Whittling Down the Possibilities: Identifying an Unknown Using Molecular Dipole Moment, Solubility, Density, and Boiling Point Data 224 Experiment 5 Recrystallization and Melting Points: Recrystallization of Adipic and Salicylic Acids 230 Experiment 6 Recrystallization and Melting Points: Recrystallization of an Unknown Solid and Decolorization of Brown Sugar 236 Experiment 7 Thin Layer Chromatography (TLC) 241 Experiment 8 Identification of an Adulterated Herb or Spice by Thin Layer Chromatography (TLC) 246 Experiment 9 What Do You Take for Pain? 253 Experiment 10 Nucleophilic Substitution Reactions of Alkyl Halides 257 Experiment 11 Isolation of Trimyristin from Nutmeg 261 Experiment 12 The MagtrieveTM Oxidation of 4-Chlorobenzyl Alcohol, A Solvent-Free Reaction 268 Experiment 13 The Sodium Borohydride Reduction of Benzil and Benzoin 273 Experiment 14 The Grignard Reaction: The Preparation of 1,1-Diphenylethanol 278 Experiment 15 The Asymmetric Dihydroxylation of trans-Stilbene 285 Experiment 16 Some Chemistry of a-Pinene Oxide 291 Experiment 17 A Dehydrogenation/Hydrogenation Reaction 296 Experiment 18 The Friedel-Crafts Reaction 303 Experiment 19 Microwave Heating of Organic Compounds 307 Experiment 20 The Reaction of 1,1-Diphenylethanol on Clay in the Presence of Microwave Radiation 312 Experiment 21 The Wittig Reaction 316 Experiment 22 The Suzuki Reaction 321 Experiment 23 The Crossed-Aldol Condensation 326 Experiment 24 Identifying the Structure of an Aldehyde by Qualitative Analysis 331 Experiment 25 The Benzoin Reaction 338 Experiment 26 The Diels-Alder Reaction 344 Experiment 27 Synthesis of an a,b-Unsaturated Carboxylic Acid Derivative 348 Experiment 28 The Reaction of 2-Acetylphenyl Benzoate with Potassium Hydroxide. Part I 355 Experiment 29 The Reaction of 2-Acetylphenyl Benzoate with Potassium Hydroxide. Part II 359 Experiment 30 Synthesis of 1,2,3,4-Tetrahydro-b-Carboline 363 Experiment 31 Base-Catalyzed Hydrolysis of Nicotinonitrile Using an Anion-Exchange Resin 367 Experiment 32 Reactions of Salicylamide 371 Experiment 33 The Hunsdiecker Reaction 377 Experiment 34 The Investigation of the Mechanism of a Reaction 381 Experiment 35 Monoterpenes and the Ritter Reaction 385 Experiment 36 Chemoselectivity in Transfer-Hydrogenation Reactions 389 Enjoy and Seed!!

udp://tracker.openbittorrent.com:80
udp://open.demonii.com:1337
udp://tracker.coppersurfer.tk:6969
udp://exodus.desync.com:6969

indiaman (2011-10-10)

Thanks rosie for this wonderful book.